[1]魏国锋1,2,张秉坚1,等.“二次生石灰”的微结构及作为文物加固剂的应用研究[J].西安建筑科技大学学报:自然科学版,2011,43(04):588-593.[doi:DOI:10.15986/j.1006-7930.2011.04.008]
 ,,et al.Microstructure and application study of secondary calcinedlime as consolidant for cultural relics[J].J.Xi’an Univ. of Arch. & Tech.:Natural Science Edition,2011,43(04):588-593.[doi:DOI:10.15986/j.1006-7930.2011.04.008]
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“二次生石灰”的微结构及作为文物加固剂的应用研究()
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西安建筑科技大学学报:自然科学版[ISSN:1006-7930/CN:61-1295/TU]

卷:
43
期数:
2011年04期
页码:
588-593
栏目:
出版日期:
2011-08-31

文章信息/Info

Title:
Microstructure and application study of secondary calcined
lime as consolidant for cultural relics
文章编号:
1006-7930(2011)04-0588-06
作者:
魏国锋1张秉坚1方世强3姚政权4
(1.浙江大学文物与博物馆学系,浙江杭州310027;2.浙江大学化学系,浙江杭州310027;
3.浙江工业大学化学工程与材料学院,浙江杭州310014;4.安徽省文物考古研究所,安徽合肥230026)
Author(s):
WEI Guo-feng1ZHANG Bing-jian1FANG Shi-qiang2YAO Zheng-quan3
(1.Department of Cultural Relics and Museology,Department of Chemistry,Zhejiang University,Hangzhou 310027,China;
2.School of Chemical Engineering and Materials,Zhejiang University of Technology,Hangzhou 310014,China;
3.Anhui Provincial Institute of Archaeology and Cultural Relics,Hefei 230026,China)
关键词:
 二次生石灰糯米灰浆土遗址加固
Keywords:
 secondary calcined limesticky rice-lime mortarearthen siteconsolidatio
分类号:
K85
DOI:
DOI:10.15986/j.1006-7930.2011.04.008
文献标志码:
A
摘要:
 在研究二次生石灰微结构的基础上,探讨了以二次生石灰为基础胶结材料用于古代建筑和土遗址加
固保护的可行性.二次生石灰的SEM 观察结果表明:氢氧化钙经高温(650℃)锻烧以后,脱水成为一种直径
为50nm、长度为200nm左右的针状纳米氧化钙;将这种纳米氧化钙消化后,会成为一种粒径在200~300
nm左右、大小十分均匀的扁平椭圆状纳米氢氧化钙颗粒.同时,研究表明,二次生石灰的纳米级粒径和高反
应活性,可以提高二次生石灰糯米灰浆的机械性能,并使二次生石灰-乙醇分散液具有良好的渗透性,较好地
解决了传统石灰水加固剂溶解度较小和渗透性较差的问题,从而为土石砖等不可移动文物的基于传统石灰
的加固技术提供了新的途径.
Abstract:
On the basis of study on microstructure of secondary calcined lime,this paper probes into applications of secondary
 calcined lime in conservation of cultural relics.SEM observations show that Ca(OH)2is transformed into a kind of acicular
 CaO with diameter 50nm and length 200nm after being calcined,and this nanosized secondary CaO is transformed
into an oval platelike Ca(OH)2 with size 200-300nm after slaked.Meanwhile,research results indicate that nanosized
particles and high reactivity of secondary calcined lime are responsible for superior properties of sticky rice-lime mortar
and high permeability of Ca(OH)2-alcohol dispersions

参考文献/References:

References
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备注/Memo

备注/Memo:
收稿日期:2010-09-08  修改稿日期:2011-06-03
基金项目:国家科技支撑计划基金资助项目(2010BAK67B16);浙江省文物保护专项基金资助(2007-197);中国博士后科学基金资
助(20100471728)
作者简介:魏国锋(1975-),男,陕西西安人,讲师,博士后,主要从事文物保护研究.
更新日期/Last Update: 2015-11-05